国产T23钢焊缝区显微组织分析

对国产T23钢焊条电弧焊接头焊缝区显微组织进行了研究。结果表明,根部焊道焊态下的组织由等轴铁素体和粒状贝氏体组成,经740℃和760℃回火后为粒状贝氏体和条状铁素体组织,在其基体上有弥散分布的点状析出物。覆盖焊道焊态下组织由粒状贝氏体和少量铁素体组成,740℃和760℃回火时为回火贝氏体组织,在690~740℃回火后形成少量聚集的粒状物,当回火温度为760℃时该粒状物分解、消失。过热区焊态下的组织由粒状贝氏体和条状马氏体组成,回火温度在690~740℃时,晶界显现,晶粒有所长大,并有大量粒状物在晶界处出现;经760℃回火处理后,原奥氏体晶界模糊、不连续,表现为回火贝氏体和回火索氏体组织,尺寸不一的点状析出物分布于基体上。     

Ag-4wt％TiB2复合材料复压复烧工艺

采用粉末冶金法制备了Ag-4％TiB2复合材料,研究了复压复烧工艺对Ag-4％TiB2复合材料组织和性能的影响.结果表明:复压复烧可改善第二相增强颗粒在基体银中的分布,使组织更加致密.随着保压时间的延长,Ag-4％TiB2复合材料的致密度、硬度和导电率呈先上升后下降的趋势;保压120s时,该复合材料的致密度、硬度和导电率达到最大值,分别为85％、115HB和50％IACS.与未复压复烧相比,Ag-4％TiB2复合材料的致密度、硬度和导电率分别提高了5.6％、6.48％和11.53％.     

碳纳米管的镍铜复合金属镀层及其抗电磁波性能

利用酸处理技术对CNT进行了改性处理。应用化学镀层法对改性后的CNT镀镍、铜及镍铜混合镀层技术进行了一系列研究。通过TG、XRD、SEM等分析表明,通过控制镀层处理的工艺条件,可以在CNT表面均匀原位生长出金属镀层,在一定条件下可形成纳米级稳定结构组成的镀层金属,而不同的金属材料形成的金相结构和分布状态有所不同。对镀层的碳纳米管材料采用四电极法和波导管法进行导电与电磁屏蔽性能测试,分析证明,复合金属镀层的电导率为17.3S/cm,电磁波屏蔽率为71dB,达到了目前国内外同类材料应用性能的优异水平。      

A new way of manufacturing high resolution optical encoders by nanoimprint lithography

A process based on nanoimprint lithography is proposed to manufacture linear encoders with a pitch below 1 μm. A phase scale and a read head were manufactured by pattern transfer on silicon and glass, respectively. The process developed points out that this technology may be suitable for mass produced encoders with a very high resolution and/or accuracy in the nanoscale range.     

粉末冶金法制备CrFeNiCuMoCo高熵合金的组织与性能

利用粉末冶金法制备CrFeNiCuMoCo高熵合金,用带有能谱的扫描电子显微镜(SEM/EDS)、X射线衍射仪、显微/维氏硬度计、电化学工作站、材料试验机等对CrFeNiCuMoCo高熵合金组织结构进行分析并测试其硬度、耐蚀性和压缩性能.结果表明:CrFeNiCuMoCo高熵合金组织形貌简单;物相主要由FCC和BCC两相组成,Mo元素和Cu元素在合金中存在偏析现象;合金的耐蚀性能优异,与304不锈钢相比,自腐蚀电流密度减小1个数量级;组元间原子半径的差异导致较大的晶格畸变,阻碍位错的运动,使得固溶强化效应增强;Mo元素起到细化晶粒作用,使该合金具有较高的硬度和抗压强度,合金硬度为485 HV,抗压强度约为1 385MPa;断裂类型为脆性解理断裂.     

Processing and phase separation of LSMO-based multiferroic composite ceramics

In this paper, the effect of processing conditions on phase separation and crystal structure of (x) La_0.625Sr_0.375MnO₃–(1 − x) LuMnO₃ composite system was studied by XRD and SEM. The results confirm that there is a solid solution of monoclinic phase of space group P112₁/a in this system, i.e. (La_0.625Sr_0.375)_x Lu_1−xMnO₃ is formed for x = 0.980–1.0. For 0 < x ≤ 0.975, the immiscibility region shows clear separation of both La-rich and Lu-rich phases. The optimal preparation conditions were found for this system: sintering at 1250 and 1350 °C for samples of monoclinic La-rich phase and for the immiscibility region, respectively.